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Herein is described a mild and effective iodination method using bis-(trifluoroacetoxy)iodobenzene-iodine as reagent to be applied to electron deficient heterocyclic systems (protected indoles, coumarin…) Moreover, sensitive protecting groups such as acetyl and tert-butyldimethylsilyl were found to be stable under the new iodination reaction conditions. In the presence of iodine and bis (trifluoroacetoxy)iodobenzene, sensitive and deactivated substrates were iodinated in high yield.
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