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This paper presents high-performance micropreconcentrators (muPCs) aimed at breath analysis and a method for eliminating unwanted species from breath samples by using a two-step preconcentration procedure. The muPC consists of embedded high aspect-ratio three-dimensional (3-D) micro pillars coated with an adsorbent polymer. The silicon-glass die has outer dimensions of 7 mm times 7 mm, total inner surface area of ~ 10 m
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