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J. Chem. Eng. Data In Journal of Chemical & Engineering Data, Vol. 52, No. 1. (9 November 2006), pp. 235-238, doi:10.1021/je060358w Key: citeulike:11923465
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The solubility of the sesquiterpene alcohol patchoulol in supercritical carbon dioxide was measured at pressures (P) ranging from 10.0 MPa to 25.0 MPa and temperatures (T) of 40.0 and 50.0 °C using a simple microsampling-type apparatus with a 100.5 ?L sample loop to remove aliquots for off-line analysis. The system was first validated using vanillin with off-line spectrophotometric analysis, then utilized for patchoulol measurements with off-line GC?MS analysis. The measured solubility of patchoulol in supercritical CO2 ranged from mole fractions of 0.43 ? 10-3 at 10.0 MPa and 50.0 °C to mole fractions of 9.4 ? 10-3 at 25.0 MPa and 40.0 °C.
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